Download Advances in Lipid Methodology. Volume 4 by W. W. Christie (Auth.) PDF

By W. W. Christie (Auth.)

This can be the fourth quantity of an occasional sequence of evaluation volumes facing features of lipid method. As with the 1st 3 volumes, themes were chosen which were constructing speedily lately and feature a few significance to lipid research. The authors are all best overseas experts.

Topics coated comprise: research of plant lipoxygenase metabolites, preparative high-performance liquid chromatography of lipids, structural research of fatty acids, and research of strong isotopes in lipids, between others

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Lipids, 31, 803-809 ( 1996). Chan,H. -S. , Lipids, 12, 99-104 (1977). J. and Suggs,J. , 2647-2650 ( 1975). B. , J. Org. , 48, 4156-4158 (1983). Ratcliffe,R. , J. Org. , 35, 4000-4002 (1970). Gardner,H. J. , Lipids, 27, 686-689 (1992). Takamura,H. and Gardner,H. , Biochim. Biophys. Acta, 1303, 83-91 (1996). C. , Plant PhysioL, 46, 445-453 (1970). Gardner,H. , J. , 11, 311-321 (1970). , Miersch,O. , Lipids, 23, 521-524 (1988). Hamberg,M. , Arch. Biochem. , 276, 518-526 (1990). C. , Lipids, 14, 734-740 ( 1979).

Interpretation of the mass spectra of various ITTMS fatty methyl esters has been published [155]. 3, references are given for spectra of LOX metabolites. iii) Infrared and ultraviolet spectroscopy. Although infrared (IR) and UV spectroscopy are less useful than their NMR and MS counterparts, these data can complete or confirm some useful information about structure. Useful IR absorbances are (cm- 1): hydro(pero)xyl, broad 3150-3620; isolated trans-double bond, 965-980; trans,trans-diene conjugation, 985; cis,trans-diene conjugation, 950 and 985; trans-epoxide, 880-890 (the cis-epoxide absorbance is not useful because it is very weak at about 825-850); aldehyde, medium at 27202730; ketone/aldehyde, about 1700-1720 (usually overlaps ester carbonyl at 1740 as a broad absorption); a,/j-unsaturated carbonyl, 1630-1640 and 1700.

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